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(Solved): Synthesis: Preparation of Vanillyl Alcohol by Sodium Borohydride Reduction. In your lab notebook, wr ...
Synthesis: Preparation of Vanillyl Alcohol by Sodium Borohydride Reduction.
In your lab notebook, write a brief analysis containing the following items. When finished, "scan" and upload to Gradescope. - Print your spectra and tape them in your lab notebook. - Draw the structure of your molecule on your infrared spectrum. Label any important diagnostic peaks. Be specific with your labels! 39 - Print your NMR spectrum and tape it into your lab notehook. Draw the structure of vanillyl alcohol on the spectrum, and label which peak corresponds to which proton. - Comment on your results. Specifically: - Based on the melting point analysis, did your experiment work, and was your product pure? Explain your reasoning. - Based on the NMR spectrum, did your experiment work, and was your product pure? Explain your reasoning, - Based on the IR spectrum, did your experiment work, and was your product pure? Explain your reasoning.
Preparation of Vanillyl Alcohol by Sodium Borohydride Reduction is performed over vanillin with 0.1 M NaOH. Find the image file for the reaction. This is a simple reduction of the aldehyde group to